By Richard W. Weiss
Read Online or Download Compounds of Germanium, Tin and Lead Including Biological Activity and Commercial Application: Covering the Literature from 1965 to 1968 (Organometallic Compounds) PDF
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Extra resources for Compounds of Germanium, Tin and Lead Including Biological Activity and Commercial Application: Covering the Literature from 1965 to 1968 (Organometallic Compounds)
G) Ana1. detn. by fusion and vo1umetrie titration (265). (h) Rxn. t. (112); po1arographie reduetion (112). * Numbers in parenthesis refer to pages in main volume. 1. R M~GeR Formu1a* Tab1e 2. o ...... p-C6~Ph Et (7) n-Pr (7) i-Pr n-Bu Ph (8) CH2 Ph (PhCH2 ) 2GeBu2 (PhCH2 )sGeEt (PhCH2)SGeBu n-Bu (8) i-Pr n-Pr (8) Et (8) R = CH2Ph MeGeRS R Me2GeR2 Formu1a* Tab1e 2 Continued - Ph2 Ge - ~Ge - RsGeH IIA IIA IIA lIIA lA IVC lA IVA - ~Ge IVC - RsGeH (j) IVB - RsGeH VIA (d) IB, IIA IB, IIA VIA (d) IB, IIA ID - MeGeIs lA ID - Me2GeC12 IIB - Me2GeC12 ID - Ph2GeX2 (i) IVA IVB IB, IB, IB, lA IVD Synth.
9824, GLC 1494 1494 1495 1495 2426 832 467,1798 2426 2425 2425 1798 1798 2425 2428 (524). 4. (a) CH2:CHCMe:CH2 used as diene (1550). (b) By-prod. in synth. (e) Rxn. prod. was not sepd. (d) IR and NMR speetra (1041-2). (e) Crude rxn. prod. reaets with CF3 C02H ~ CsHa (1041-2). (f) Synth. from 1,3-eye10hexadieneo (g) Synth. from 1,4-cye10hexadiene. (h) Rxn. with CFSC02H ~ MesGe02CCFs + R'H (1041-2). (i) NMR speetrum (1526). (j) Mixture of endo-, exo-norborney1-GeMes and nortrieye1eny1-GeMes, not separab1e by GLC, ratio by NMR = 75:15:10 (1041-2).
O~ 160°, far IR (105) and mass (1109) spectra. Other nonfunctiona1 tetraorganogermanes with two different organie substituents are compi1ed in Tab1e 2. 8 \0 (7) p-Ce~Ph n- CeH13 e. CSH9 (7) CHEtCH2Ph i-Bu t-Bu CH2 CHCH2 CH2 (7) CHPrPh n-Bu (7) i-Pr n-Pr (7) = Et IllE IlB - IlC ID - ID IlC M~GeBr M~GeI M~GeI ID - M~CGeC13 ID - BuGeXs ID - M~GeC1 IA VIA (d) ID - PrGeXs IB, lIA ID - i-PrGeIs IB, IlA lE Synth. Method** 14 74 30 71 21 67 66 62 Yie1d m. 515~-62 (f) b. 5° GLC (b) b. 9816 GLC (491, 492) (e, e) b.