Inorganic Syntheses, Volume 33 by Dimitri Coucouvanis

By Dimitri Coucouvanis

The Inorganic Syntheses sequence offers inorganic chemists with certain and foolproof strategies for the practise of vital and well timed compounds. quantity 33 comprises provocative contributions on syntheses of chosen supramolecules, beneficial reagents/ligands, strong kingdom materials/clusters, and different compounds of common curiosity.

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89). B. a-PENTASODIUM DODECATUNGSTOALUMINATE a-Na5[AlW12O40] This procedure converts a mixture of - and -H5[A1W12O40] to $ 95% -Na5[A1W12O40]. The isomer, because of its lower solubility, is easily separated from the residual amount of isomer. 9-g sample of H5[A1W12O40] 3. Dodecatungstoaluminic Acid and Its Derivatives 23 is dissolved in 65 mL of water and filtered if cloudy. 5 mL) and is then heated at reflux for 3 days. At this point, the solution typically contains about 95% -[A1W12O40]5À (with 5% , determined by 27A1 NMR).

Chem. 55, 325 (1964); (d) G. Denti, S. Serroni, L. Sabatino, M. Ciano, V. Ricevuto, and S. Campagna, Gazz. Chim. Ital. 121, 37 (1991). 6. H. A. Goodwin and F. Lions, J. Am. Chem. Soc. 81, 6415 (1959). 7. Emission spectra have been obtained with a Perkin-Elmer LS-50 spectrofluorimeter equipped with a Hamamatsu R958 phototube. Data are uncorrected for spectral sensitivity of the phototube. 3. DODECATUNGSTOALUMINIC ACID AND ITS MONOLACUNARY AND MIXED-ADDENDUM DERIVATIVES Submitted by JENNIFER J. COWAN,* CRAIG L.

J. Conklin, G. T. Yee, and S. T. Weintraub, Chem. Eur. J. 1, 528–537 (1995). 18. A. J. Bard and L. R. Faulkner, Electrochemical Methods, Wiley, New York, 1980. 19. N. G. Conelly and W. E. Geiger, Chem. Rev. 96, 877 (1996). 20. E. S. -S. Chan, and A. C. Wahl, J. Phys. Chem. 79, 2049–2051 (1975). 2. A LUMINESCENT DECANUCLEAR RUTHENIUM(II) POLYPYRIDINE COMPLEX: A CONVERGENT APPROACH TO A DENDRITIC STRUCTURE EMPLOYING THE ‘‘COMPLEXES AS METALS/COMPLEXES AS LIGANDS’’ SYNTHETIC STRATEGY Submitted by SCOLASTICA SERRONI,*,y SEBASTIANO CAMPAGNA,* FAUSTO PUNTORIERO,* ALBERTO JURIS,z GIANFRANCO DENTI,y VINCENZO BALZANI,z and MARGHERITA VENTURIz Checked by DARON JANZEN and KENT R.

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